期刊
ORGANIC LETTERS
卷 14, 期 17, 页码 4650-4653出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol302098u
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资金
- TAMOP project [4.2.1/B-09/1/KONV-2010-0007]
- European Union
- European Social Fund
- Hungarian Research Fund [OTKA K 79126]
Free-radical hydrothiolation of the endocyclic double bond of enoses is reported. Reaction between 2-acetoxy-D-glucal and a range of thiols including amino acid, peptide, glycosyl thiols, and sugars with primary or secondary thiol functions gave S-linked alpha-glucoconjugates and S-disaccharides with full regio- and stereoselectivity. Addition of glycosyl thiols to a 2,3-unsaturated glycoside also proceeded with good selectivity and afforded a series of 3-deoxy-S-disaccharides.
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