期刊
ORGANIC LETTERS
卷 14, 期 8, 页码 2150-2153出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol300673m
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资金
- New Mexico State University
- NMSU-MBRS Research Initiative for Scientific Enhancement [NIH R25GM061222]
- NMSU-Howard Hughes Medical Institute [52006932]
The first asymmetric total synthesis and determination of the absolute configuration for the neuroactive marine macrolide palmyrolide A is described. The highlight of the synthesis is macrocyclization via trans-enamide formation catalyzed by copper(I) iodide and cesium carbonate. Comparison with the authentic spectral data confirms the synthesis of (+)-ent-palmyrolide A.
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