期刊
ORGANIC LETTERS
卷 15, 期 1, 页码 192-195出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol303253h
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资金
- Givaudan
- Wild Fund
- University of York
- EU/Celtic Catalysts (Marie-Curie Transfer of Knowledge grant)
The first examples of the asymmetric synthesis of P-stereogenic vinylic phospholene boranes are described. The synthetic approach is concise and flexible. The route involves (i) asymmetric deprotonation-allylation of a dimethyl phosphine borane; (ii) telescoped regioselective deprotonation, paraformaldehyde trapping, and hydroxyl group elimination to give a diene; and (iii) ring-closing metathesis.
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