期刊
ORGANIC LETTERS
卷 14, 期 12, 页码 3130-3133出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol3012106
关键词
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资金
- Centre National de la Recherche Scientifique (CNRS)
- Region Aquitaine
- University of Bordeaux
- European Union [Marie Curie PEOPLE-2010-IEF-273224-FOLDAPOP]
- ImmuPharma (CIFRE)
A practical and efficient microwave-assisted solid-phase method for the synthesis of N,N'-linked oligoureas and related amide/urea hybrid oligomers, featuring the use of succinimidyl (2-azido-2-substituted ethyl) carbamate monomers, is reported. The rate enhancement of urea formation under microwave irradiation combined with the mild conditions of the phosphine-based azide reduction makes this approach very effective for routine synthesis of oligoureas and possibly for library production.
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