期刊
ORGANIC LETTERS
卷 13, 期 19, 页码 5016-5019出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol201779n
关键词
-
资金
- National Science Foundation of China [20972057, 20102039]
A metal-free novel, simple, and highly efficient method for the direct C2-alkylation of azoles with alcohols and ethers has been developed on the basis of an oxidative C-H activation process. The dehydrogenative C-C cross-coupling reactions of alpha-position sp(3) C-H in alcohols and ethers with the 2-position sp(2) C-H in azoles proceeded smoothly in the presence of tert-butyl hydroperoxide (TBHP) under neat reaction conditions, which generated the corresponding products in good yields.
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