期刊
ORGANIC LETTERS
卷 13, 期 9, 页码 2150-2152出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol200379r
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资金
- Minister dell'Istruzione, dell'Universita e della Ricerca (MIUR)
- Universita degli Studi di Perugia [RBFR08TTWW, RBFR08J78Q]
This report concerns Lewis acid catalyzed enantioselective sulfa-Michael addition in neutral water by using a very efficient Sc(OTf)(3)/bipyridine 1 catalytic system. It is noteworthy that the protocol presented employs water as a reaction medium and allows us to obtain very high stereoselectivity and satisfactory yields for beta-keto sulphides deriving from aliphatic thiols. The recovery and reuse of both the aqueous medium and the catalytic system is also reported.
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