期刊
ORGANIC LETTERS
卷 13, 期 2, 页码 328-331出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol102812c
关键词
-
资金
- Ministerio de Ciencia e Innovacion of Spain
A convenient, efficient synthesis of 1,2,4-triazolines from alpha-isocyano esters/amides and azodicarboxylates is presented. The developed reaction cascade is based on a base-catalyzed hydrazination-type reaction followed by a subsequent cyclization providing the triazolines in good to excellent yields (75-99%). Phosphine-catalyzed and preliminary asymmetric phase-transfer catalysis approaches have also been investigated.
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