期刊
ORGANIC LETTERS
卷 13, 期 24, 页码 6386-6389出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol202593g
关键词
-
资金
- Ministry of Education, Science, and Technology through the National Research Foundation of Korea [2010K001050, 2010-0018937]
Highly conjugated azines were prepared by solid state grinding of solid hydrazine and carbonyl compounds such as aldehydes and ketones, using a mortar and a pestle. Complete conversion to the azine product is generally achieved at room temperature within 24 h, without using solvents or additives. The solid-state reactions afford azines as the sole products with greater than 97% yield, producing only water and carbon dioxide as waste.
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