期刊
ORGANIC LETTERS
卷 13, 期 19, 页码 5398-5401出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol202306d
关键词
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资金
- JSPS [22249001]
- MEXT [2105, 22106538]
- Grants-in-Aid for Scientific Research [21590012, 23790015, 22249001, 22106538] Funding Source: KAKEN
The first total synthesis of oxazolomycin A, a structurally novel oxazole polyene gamma-lactam/beta-lactone antibiotic, is described. Key features Include the stereocontrolled construction of the right-hand heterocyclic core by taking advantage of an In(III)-catalyzed Conia-ene type cyclization and the asymmetric synthesis of the left-hand segment starting with a Cinchona alkaloid-catalyzed cyclocondensation of an aldehyde with an acid chloride.
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