期刊
ORGANIC LETTERS
卷 13, 期 24, 页码 6374-6377出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol2026747
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资金
- Ministry of Education, Culture, Sports, Science and Technology of Japan
The first enantioselective Neber reaction of beta-ketoxime sulfonates catalyzed by a bifunctional thiourea has been developed. The reaction proceeds stereoselectively with 5 mol % of the catalyst to give the 2H-azirine carboxylic esters in good yields with up to 93% ee. In addition, the resulting azirines can be successfully employed in the stereoselective synthesis of di- and trisubstituted aziridines.
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