期刊
ORGANIC LETTERS
卷 14, 期 1, 页码 114-117出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol202895u
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资金
- Naito Foundation
- Nagase Science and Technology Foundation
- Suntory Institute for Bioorganic Research
- Global COE from MEXT
- Japan Society for Promotion of Science-Asian Core Program (JSPS-ACP) on Cutting-Edge Organic Chemistry in Asia
- National Research Council of Thailand (NRCT)
- Chulabhorn Research Institute (CRI)
- Grants-in-Aid for Scientific Research [24580161, 20380067, 22780102] Funding Source: KAKEN
Two possible diastereomers of the indole moiety of sespendole were synthesized from 3-hydroxy-4-nitrobenzaldehyde in a highly stereoselective manner. Comparison of H-1 and C-13 NMR spectra of the two synthetic materials with those sespendole leads us to propose that the relative stereochemistry of the epoxyalcohol is syn.
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