期刊
ORGANIC LETTERS
卷 12, 期 10, 页码 2214-2217出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol100540p
关键词
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资金
- National Natural Science Foundation of China [20732003, 20702033]
- PC-SIRT [IRT0846]
- National Basic Research Program of China [2010CB833300]
The N,N'-dioxide-Cu(OTf)(2) complexes were applied in,the asymmetric amination reaction of N-acetyl enamides with dialkyl azodicarboxylate, giving the corresponding products in good yields with high enantioselectivities (up to 91% ee). Precursors of vicinal diamine were readily obtained with excellent diastereoselectivities (>95:5) by NaBH4 reduction.
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