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卷 12, 期 22, 页码 5294-5297出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol102296t
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- HEC (Pakistan)
- AstraZeneca
- Pfizer
The tricyclic spirochroman core of dihypoestoxide has been synthesized from geranoic acid in seven steps using a hetero-Diels-Alder cycloaddition as a key step, thus providing support for the proposed biosynthesis of the natural product. Furthermore, analysis of the C-13 NMR data obtained for all four diastereoisomers of the synthetic spirochroman core has allowed us to propose a full stereochemical assignment for dihypoestoxide.
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