期刊
ORGANIC LETTERS
卷 11, 期 23, 页码 5494-5496出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol9023453
关键词
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资金
- Thailand Research Fund
- Center for Innovation in Chemistry (PERCH-CIC)
- Commission on Higher Education, Thai Ministry of Education
Nucleophilic cleavage of enantiomerically pure 1,2-cyclic sulfamidates with phenol, aniline, and thiophenol nucleophiles, followed by a Mitsunobu reaction, including use of a o-quinomethide variant of this process, provides an entry to substituted 1,4-tetrahydrobenzoxazepines, benzothiazepines, and benzodiazepines. Application of this methodology to 1,3-cyclic sulfamidates affords a parallel entry to the analogous substituted 1,5-benzoxazocines and 1,5-benzodiazocines.
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