期刊
ORGANIC LETTERS
卷 11, 期 14, 页码 2976-2979出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol9009859
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资金
- BBSRC SCIBS initiative [BBE0140891]
- BBSRC strategic research [BBSSH200511988]
- BBSRC [BB/E014089/1] Funding Source: UKRI
- Biotechnology and Biological Sciences Research Council [BB/E014089/1] Funding Source: researchfish
Two new and complementary synthetic strategies for 5'-N-chloroethylamino-5'-deoxyadenosines are presented. Additionally, the reaction kinetics of their conversion into aziridines under typical enzyme assay conditions is reported using time-resolved NMR spectroscopy. A stable photocaged derivative of 5'-N-chloroethylamino-5'-deoxyadenosine has also been synthesized, and its stability and activation In aqueous solution at physiological pH have been examined.
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