期刊
ORGANIC LETTERS
卷 11, 期 7, 页码 1511-1514出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol900103a
关键词
-
资金
- NIH [GM069559]
- Director, Office of Energy Research, Office of Basic Energy Sciences, Chemical Sciences Division, U.S. Department of Energy [AC02-05CH11231]
A method for the direct arylation of benzotriazepines is reported, employing an aryl iodide as the coupling partner, copper iodide as the catalyst, and lithium tert-butoxide as the base. A variety of electron-rich, electron-poor, and sterically hindered aryl iodides are compatible with the reaction conditions. The arylation reaction can also be performed outside a glovebox in air without a significant decrease in yield. Furthermore, convenient microwave conditions for carrying out this transformation are reported.
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