期刊
ORGANIC LETTERS
卷 10, 期 7, 页码 1433-1436出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol800255r
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资金
- NIGMS NIH HHS [GM51982, GM57878] Funding Source: Medline
Pyrrolidine enones, derived from 3-oxo pyrrolidine 2-phosphonates and a HWE reaction with aldehydes, on Luche reduction give pyrrolidine allylic alcohols. The alcohols on hydrogenation (Pd/H(2)) give cis-2,5-disubstituted pyrroliclines and on treatment with TFA-NaBH(3)CN undergo a hydroxy directed reduction to trans-2,5-disubstituted pyrrolidines.
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