期刊
ORGANIC LETTERS
卷 10, 期 17, 页码 3853-3856出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol8016484
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资金
- American Chemical Society Petroleum Research Fund
The reaction of aldehydes with trichloromethide followed by sodium borohydride or sodium phenylseleno(triethyl)borate under basic conditions affords homologated carboxylic acids in high yields. This operationally simple procedure provides a practical, efficient alternative to other homologation protocols. The approach is compatible with sensitive aldehydes including enals and enolizable aldehydes. It also offers convenient access to alpha-monodeuterated carboxylic acids.
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