4.8 Article

Twofold C-H functionalization:: Palladium-catalyzed ortho arylation of anilides

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卷 10, 期 11, 页码 2207-2210

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AMER CHEMICAL SOC
DOI: 10.1021/ol800619c

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  1. NIGMS NIH HHS [R37 GM046059, GM46059, R37 GM046059-16, R01 GM046059] Funding Source: Medline

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The ortho arylation of anilides to form biphenyls via a twofold C-H functionalization/C-C bond-forming process is described. The oxidative coupling takes place in the presence of 5-10 mol % of Pd(OAC)(2), 10-20 mol % of DMSO, and 4-11 equiv of the aryl substrate in TFA under an oxygen atmosphere. No metal-containing cocatalyst is required.

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