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Diene-titanium complexes as synthetic intermediates for the construction of three- or five-membered carbocycles

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ORGANIC LETTERS
卷 10, 期 5, 页码 777-780

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AMER CHEMICAL SOC
DOI: 10.1021/ol702917c

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It has been shown that diene-titanium complexes exhibit substrate-dependent 1,2- or 1,4-dicarbanion reactivity. On this basis, 3-cyclopentenylamines and spiro-vinylcyclopropane lactams were easily prepared by using homoallylic Grignard reagents, Ti(O-i-Pr)(4), and nitriles or cyanoesters, respectively.

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