期刊
ORGANIC & BIOMOLECULAR CHEMISTRY
卷 9, 期 3, 页码 673-675出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c0ob00850h
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资金
- Ministry of Education, Culture, Sports, Science and Technology of Japan
An efficient diastereoselective synthesis of (-)-stemoamide has been accomplished from a pyroglutamic acid derivative in eight steps and with 24% overall yield. The synthesis features an intramolecular samarium diiodide-promoted 7-exo-trig cyclization of a ketyl radical generated from the corresponding aldehyde.
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