期刊
ORGANIC & BIOMOLECULAR CHEMISTRY
卷 6, 期 10, 页码 1808-1813出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/b800884a
关键词
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Aryl thioesters of peptide segments were prepared by the conventional 9-fluorenylmethoxycarbonyl (Fmoc) strategy using a novel N-alkyl cysteine (NAC)-assisted thioesterification reaction. The peptide carrying NAC at its C-terminus was prepared by the Fmoc strategy and converted to the aryl thioester by 4-mercaptophenylacetic acid (MPAA) treatment without significant side reactions. The peptide thioester was used for the efficient preparation of 95-amino acid (AA) chemokine CCL27 by an Ag+-free thioester method.
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