期刊
TETRAHEDRON LETTERS
卷 56, 期 12, 页码 1505-1509出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2015.01.154
关键词
Aminosulfuration; Diamination; Alkenes; N-Iodosuccinimide; Aminooxygenation
资金
- Shanghai Pujiang Talent Program [11PJ1402500]
- National Natural Science Foundation of China [21171056, u1162111, u1362111]
A NIS-mediated intramolecular diamination and aminosulfuration of alkenes with N-alkyl or N-aryl thioureas is reported. A chiral cyclic thiourea was also synthesized by the methodology. The protocol is also proven to be efficient in the intramolecular diamination and/or aminooxygenation of alkenes with N-alkyl or N-aryl ureas and ones with N-carbamate sulfamides. The resulting bicyclic thiourea could be further transformed into bicyclic guanidine. (C) 2015 Elsevier Ltd. All rights reserved.
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