期刊
TETRAHEDRON LETTERS
卷 56, 期 46, 页码 6448-6451出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2015.09.148
关键词
Indium; Hydrosiloxane; Secondary amide; Secondary amine; Reduction
资金
- Ministry of Education, Culture, Sports, Science, and Technology (MEXT), Japan [25410120]
- Grants-in-Aid for Scientific Research [25410120] Funding Source: KAKEN
Described herein is that the selective reduction of aromatic/aliphatic secondary amides using a combination of InI3 and TMDS (1,1,3,3-tetramethyldisiloxane), which led to the production of the corresponding secondary amines. This reducing system showed a relatively high tolerance to a variety of functional groups, such as an alkyl, an alkoxy, a halogen, a cyano, an ether, a thioether, a heterocyclic ring, and a terminal alkene group. (C) 2015 Elsevier Ltd. All rights reserved.
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