4.4 Article

Peroxide promoted metal-free thiolation of phosphites by thiophenols/disulfides

期刊

TETRAHEDRON
卷 71, 期 41, 页码 7853-7859

出版社

PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2015.08.025

关键词

Oxidative coupling; Thiophophate; Di-tert-butyl peroxide; Metal-free; Phosphites

资金

  1. National Natural Science Foundation of China [21025207]

向作者/读者索取更多资源

A metal-free oxidative P-S bonds coupling method for the synthesis of thiophosphates with DTBP as the oxidant is established. A wide range of functionalities are tolerated in the method. This method provides a facile way to synthesize thiophophates from readily available thiophenols/disulfides and phosphites. (c) 2015 Elsevier Ltd. All rights reserved.

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