4.7 Article

Synthesis and characterization of reduced graphite oxide-polymer composites and their application in adsorption of lead

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PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.saa.2015.04.071

关键词

Reduced graphite oxide; Poly 1,5-(diaminonaphthalene); Poly 1,4-(diaminoanthraquinone); Lead; Adsorption

资金

  1. NIH-NIGMS [1SC3GM086245]
  2. Welch Foundation [L0002]

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Herein, we report the in situ polymerization of 1,5-diaminonaphthalene (15DAN) and 1,4-diaminoanthraquinone (14DAA) on the surface of reduced graphite oxide (RGO). Synthesized RGO-P15DAN and RGO-P14DAA were characterized by FTIR, Raman, SEM, TGA and XRD. The adsorption capacity and adsorptivity of the synthesized composites were investigated by Atomic Absorption Spectroscopy (AAS) using 100 ppm aqueous solution of Pb2+ ions. Further, we compared the results of the composites with those of poly 1,5-(diaminonaphthalene) (P15DAN), poly 1,4-(diaminoanthraquinone) (P14DAA), RGO, graphite oxide (GO) and graphite. Among the tested adsorbents, RGO-P15DAN demonstrated the high adsorptivity. (C) 2015 Elsevier B.V. All rights reserved.

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