期刊
NATURAL PRODUCT RESEARCH
卷 25, 期 14, 页码 1324-1333出版社
TAYLOR & FRANCIS LTD
DOI: 10.1080/14786419.2010.531017
关键词
Staurocucumis liouvillei; triterpene glycosides; liouvilloside A(4); liouvilloside A(5); sea cucumbers; 3-O-methyl-D-quinovose
资金
- Presidium of the Russian Academy of Science
- Russian Federation [3531.2010.4]
- ECOQUIM from Spain
- ACTIQUIM from Spain [REN2003-00545, CGL2004-03356/ANT, CGL2007-65453/ANT]
Two new minor triterpene glycosides, liouvillosides A(4) (1) and A(5) (2) have been isolated from the sea cucumber Staurocucumis liouvillei living in Antarctic and Sub-Antarctic waters. The structures of the new glycosides were elucidated using extensive nuclear magnetic resonance (NMR) spectroscopy (H-1- and C-13-NMR spectroscopy, H-1-H-1 COSY, 1D-TOCSY, HMBC, HSQC and NOESY), ESI-MS and MALDI TOF MS. The glycosides 1 and 2 are disulphated tetraosides having very rare 3-O-methylquinovose as terminal monosaccharide.
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