4.8 Article

Nondestructive volumetric 3-D chemical mapping of nickel-sulfur compounds at the nanoscale

期刊

NANOSCALE
卷 4, 期 5, 页码 1557-1560

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ROYAL SOC CHEMISTRY
DOI: 10.1039/c2nr11690a

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资金

  1. Energy Frontier Research Center on Science Based Nano-Structure Design and Synthesis of Heterogeneous Functional Materials for Energy Systems (HeteroFoaM Center)
  2. U.S. Department of Energy, Office of Science, Office of Basic Energy Sciences [DE-SC0001061, DE-AC02-06CH11357]
  3. National Science Foundation [CBET-1134052]
  4. Brookhaven Science Associates, LLC [DE-AC02-98CH10886]
  5. Div Of Chem, Bioeng, Env, & Transp Sys
  6. Directorate For Engineering [1134052] Funding Source: National Science Foundation

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Nano-structures of nickel (Ni) and nickel subsulfide (Ni3S2) materials were studied and mapped in 3D with high-resolution x-ray nanotomography combined with full field XANES spectroscopy. This method for characterizing these phases in complex microstructures is an important new analytical imaging technique, applicable to a wide range of nanoscale and mesoscale electrochemical systems.

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