期刊
MOLECULES
卷 17, 期 7, 页码 8174-8185出版社
MDPI
DOI: 10.3390/molecules17078174
关键词
2,3-disubstituted-1,3-benzoxazine; synthesis; chlorotrimethylsilane; fungicidal activity
资金
- National Natural Science Foundation of China [21042011]
- Hunan Provincial Education Department [10A034]
- Hunan Provincial Natural Science Foundation [11JJ3016]
- Key Laboratory of Theoretical Chemistry and Molecular Simulation of Ministry of Education [LKF0906]
A series of new 2,3-disubstituted-3,4-dihydro-2H-1,3-benzoxazines were prepared in moderate to excellent yields by aza-acetalizations of aromatic aldehydes with 2-(N-substituted aminomethyl)phenols in the presence of TMSCl. Their structures were confirmed by IR, H-1-NMR, C-13-NMR, MS and elemental analysis. The fungicidal activities of the target compounds were preliminarily evaluated, and some compounds exhibited good activity against Rhizoctonia solani.
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