期刊
MOLECULES
卷 16, 期 11, 页码 9340-9356出版社
MDPI
DOI: 10.3390/molecules16119340
关键词
alkyne; cyclocondensation; multi-component reaction; pyrazole; Sonogashira coupling
资金
- Fonds der Chemischen Industrie
A novel consecutive three-component synthesis of 3-(hetero)aryl-1H-pyrazoles via room temperature Sonogashira arylation of propynal diethylacetal used as a propargyl aldehyde synthetic equivalent has been disclosed. The final acetal cleavage-cyclocondensation with hydrazine hydrochloride at 80 degrees C rapidly furnishes the title compounds in a one-pot fashion.
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