期刊
MICROCHEMICAL JOURNAL
卷 108, 期 -, 页码 32-37出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/j.microc.2012.12.007
关键词
Biodiesel/diesel blends; Synchronous fluorescence; Gross heat of combustion; Cetane number; Color; SPA-MLR; PLS
An analytical method was developed to determine four quality parameters (Biodiesel percentage, Cetane Number, Heat of Combustion Gross and Color) in biodiesel/diesel blends through a simple synchronous fluorescence spectrum of the samples. For this purpose, chemometrics models based on fluorescence spectra and PetroSpect data obtained from mixtures of biodiesel/diesel were built. A variable selection by the successive projections algorithm (SPA) was used in order to obtain simple multiple linear regression (MLR) models based on a small subset of wavelengths. The SPA-MLR results were compared with a partial least squares (PLS) full spectrum regression. The best values found for the root mean square error of prediction using external validation were 037% (w/w) for the biodiesel in diesel, 0.5 for cetane number, 0.013 MJ/kg for heat of combustion and 0.1 for color. (C) 2012 Elsevier B.V. All rights reserved.
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