4.5 Article

Parallelization of photocatalytic gas-producing reactions

期刊

REVIEW OF SCIENTIFIC INSTRUMENTS
卷 86, 期 3, 页码 -

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AMER INST PHYSICS
DOI: 10.1063/1.4915349

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  1. School Research and Development Council at the Lebanese American University
  2. Lebanese National Council for Scientific Research [05-06-14]
  3. NSF [CHE-1012487, CHE-1418758]

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High-throughput screening has been widely utilized in the pharmaceutical and manufacturing industry targeting the development of new molecules and materials for numerous applications. To enable more rapid progress in photocatalytic water-splitting reactions, the construction of high-throughput combinatorial photoreactors enabling the parallel optimization of relevant compositions under varieties of experimental conditions seems appropriate. This contribution describes a 16-photoreactor apparatus permitting the kinetic evaluation of photocatalytic gas-producing reactions using headspace pressure, gas chromatography, and mass spectrometry operating in parallel, illustrated with molecular-based homogeneous photocatalytic H-2-generating compositions. (C) 2015 AIP Publishing LLC.

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