Microstructure and mechanical property of nano-SiCp reinforced high strength Mg bulk composites produced by friction stir processing

Friction stir processing has been applied to fabricate SiC-Mg bulk composites in this study. AZ63 magnesium alloy, a kind of commercial engineering materials, was selected as base metal. SiC nanoparticles with average size of 40 nm were selected as reinforced particles. After being ultrasonic dispersed in ethanol and friction stir processed with base metal, the SiC particles were uniformly dispersed. Friction stir processing without filling any particles was also applied to base metal as a comparison group. Microstructure evolution was observed by optical microscope and scanning electron microscope. Fine and uniform nugget zone were found both in comparison group and composite. The phases of the material were determined by X-ray diffraction. Transmission electron microscopy observation was conducted to study the condition of SIC nanoparticles. SIC particles were found both inside the grain and at the grain boundary. No micro-sized particle agglomeration was observed in the composite. Vicker hardness and tensile test were carried out to study the mechanical properties of the composite. The average Vicker hardness of the base metal, comparison group and composite were 80 Hv, 85 Hv and 109 Hv respectively. The ultimate tensile strength of the composite reached 312 MPa. Compared with 160 MPa of the as-casted Mg alloy, 263 MPa of the comparison group, the effect of nanoparticles on strength increase was significant. (C) 2012 Elsevier B.V. All rights reserved.