期刊
MATERIALS RESEARCH-IBERO-AMERICAN JOURNAL OF MATERIALS
卷 12, 期 2, 页码 139-143出版社
UNIV FED SAO CARLOS, DEPT ENGENHARIA MATERIALS
DOI: 10.1590/S1516-14392009000200005
关键词
aluminosilicate; dental cement; glass ionomer; NMR(27)Al-(29)Si
资金
- FAPESP
- CNPq
- CAPES (Brazilian research funding agencies)
Glass ionomer cements are widely employed in dentistry due to their physical, biological and mainly anti-caries properties. Glass ionomers consist of an aluminosilicate glass matrix modified with other elements, and they contain large quantities of fluorine. In this study, we report on the preparation of calcium-fluoroaluminosilicate glasses by a nonhydrolytic sol-gel route as an alternative approach to obtaining alumina-silica matrices. The glass powders were prepared via the non-hydrolytic sol-gel method, by mixing AlCl(3), SiCl(4), CaF(2), AlF(3), NaF, and AlPO(4). The powders were studied by thermal analysis (TG/DTA/DSC), photoluminescence (PL), nuclear magnetic resonance (NMR(27)Al-(29)Si), and X ray diffraction (XRD). TG/DTA/DSC analyses revealed a constant mass loss due to structural changes during the heating process, which was confirmed by NMR and PL. A stable aluminosilicate matrix with potential future application as a glass ionomer base was obtained.
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