期刊
MATERIALS RESEARCH BULLETIN
卷 55, 期 -, 页码 67-70出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.materresbull.2014.04.008
关键词
Nanostructures; Chemical synthesis; Crystal growth
资金
- National Natural Science Foundation of China [51172260, 51121064]
- Science and Technology Commission of Shanghai [11nm0506600]
Hydroxyapatite nanorods are synthesized by the hydrothermal method using biocompatible biomolecule pyridoxal-5'-phosphate (PLP) as a new organic phosphorus source. In this method, PLP biomolecules are hydrolyzed to produce phosphate ions under hydrothermal conditions, and these phosphate ions react with pre-existing calcium ions to form hydroxyapatite nanorods. The effects of experimental conditions including hydrothermal temperature and time on the morphology and crystal phase of the products are investigated. This method is simple, surfactant-free and environmentally friendly. The products are characterized by X-ray powder diffraction, scanning electron microscopy, transmission electron microscopy, Fourier transform infrared (FTIR) spectroscopy, and thermogravimetric (TG) analysis. (C) 2014 Elsevier Ltd. All rights reserved.
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