期刊
MATERIALS LETTERS
卷 133, 期 -, 页码 1-4出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/j.matlet.2014.06.030
关键词
Luminescence; Phosphors; Sol-gel preparation; Carbon-free; WLEDs; LuAG
资金
- National Basic Research Program of China [2012CB933103]
- National Natural Science Foundation of China [51371154]
Ce3+-doped lutetium aluminum garnet (LuAG) phosphors have been successfully synthesized by a facile carbon-free sol-gel method without using any organic gelling agent. Phase transitions from gel to LuAG were well investigated by X-ray diffraction and thermal analysis. The results confirmed that a pure LuAG phase can form at around 920 degrees C by directly crystallizing from amorphous material. Particle size of the LuAG phosphor can be controlled by adjusting the heat treatment process; therefore, both nano and micron-scale products can be obtained and they are suitable for the fabrication of laser scintillators and white light emitting diodes, respectively. Agglomeration can be observed in the nano-sized phosphor. For the micron-sized LuAG, a two-step process was used to avoid hard agglomeration. Particles of the obtained micron-sized phosphor are uniform and well-dispersed. Luminescence properties of the phosphors were characterized. Relative intensity of the micron-sized product is comparable with commercial phosphor. (C) 2014 Published by Elsevier B.V.
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