期刊
MATERIALS LETTERS
卷 107, 期 -, 页码 162-165出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/j.matlet.2013.05.133
关键词
Nanocomposites; ZnO nanorods; Polymers; Surface-initiated; ATRP
资金
- Postdoctor Innovation Project [201102020]
- Science and Technology Planning Project of Shandong Province [ZR2011BL004, J10LB54]
- Excellent Talents Program of Taishan University [Y07-2-05]
One-dimensional ZnO/polymer nanohybrids were prepared from ZnO nanorods via surface-initiated atom transfer radical polymerization (ATRP) technique. Firstly, well-defined ZnO nanorods were synthesized by the solvent-thermal method. Subsequently, the ZnO nanorods were functionalized with 3-aminopropyl-trimethoxysilane, which was converted to ATRP initiators by the esterification of them with 2-bromoisobutyryl bromide. ZnO/polymer nanocables were then obtained in an ATRP of 2-hydroxyethyl methacrylate with CuBr/2,2-bipyridine as the catalyst system. X-ray photoelectron spectroscopy, Transmission electron microscopy, and Thermogravimetric analysis are all used to characterize the as-prepared ZnO-polymer hybrids. This protocol provides a practical and flexible approach to integrate multifunctionalities on a variety of nanostructured substrates. (C) 2013 Elsevier B.V. All rights reserved.
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