期刊
MATERIALS CHEMISTRY AND PHYSICS
卷 112, 期 3, 页码 1024-1028出版社
ELSEVIER SCIENCE SA
DOI: 10.1016/j.matchemphys.2008.07.020
关键词
Zinc oxide; Synthesis; Nanostructures; X-ray diffraction; Electron microscopy
资金
- National Natural Science Foundation of China [90306001, 20273068, 60778040]
Submicrometer zinc oxide (ZnO) with different morphologies including spindle-like, pencil-like, branch rod-like and frizzy flower-like shapes, have been hydrothermally synthesized in mixed solvents of ethanol and water at 140 degrees C. It was found that the volumes of added ammonia, surfactant (cetyltrimethylammonium bromide, CTAB), and mixed solvent play crucial roles in morphological control of ZnO nanostructures. Increasing the volume of ammonia added to the reaction system, the shape of ZnO evolves from spindle into branch rod-like. Synergetic influence between CTAB and ammonia can only be observed at high concentration of ammonia. (C) 2008 Elsevier B.V. All rights reserved.
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