期刊
MATERIALS CHEMISTRY AND PHYSICS
卷 108, 期 2-3, 页码 188-191出版社
ELSEVIER SCIENCE SA
DOI: 10.1016/j.matchemphys.2007.10.007
关键词
chalcogenides; chemical synthesise; electron microscopy (STEM TEM and SEM)
MoS2 with different morphologies was prepared by hydrothermal synthesis. The combined techniques of X-ray diffraction, energy dispersive X-ray spectrum, field emission scanning electron microscope, transmission electron microscope, Raman spectra and thermal analysis in air were used for characterization of the as-obtained MoS2. Effects of aging period on the morphology were investigated. The particles grew more spherical with aging period prolonging and flowers were obtained at much longer aging period. (c) 2007 Elsevier B.V. All rights reserved.
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