期刊
MATERIALS CHARACTERIZATION
卷 60, 期 5, 页码 451-455出版社
ELSEVIER SCIENCE INC
DOI: 10.1016/j.matchar.2008.10.003
关键词
Nanoparticle powder; Mechanical alloying process; CuInSe2 thin films
类别
资金
- CMEP Tassili project [Ndegree.08MDU733]
This work studies the properties of CuInSe2 (CIS) thin films obtained from nanoparticle powder. The samples were prepared by direct thermal evaporation of ball milled powder from a tungsten crucible onto precleaned glass substrates, using a BALZERS coating unit. The as deposited films were annealed in a vacuum at different temperatures. The composition, structure, morphology and optical properties of these samples have been investigated. X-ray diffraction (XRD) results showed that the CuInSe2 phase may be prepared by mechanical alloying method. The crystallites of the CIS powder were found to be partially copper-rich. The as-deposited film was polycrystalline in nature having chalcopyrite structure as a mainly phase. The surface morphology is homogeneous across the surface. Expected optical properties (Eg=1.04 eV, alpha approximate to 10(4) cm(-1)) and near stoichiometric composition (Cu: 23.62 at.%, In: 24.35 at.% and Se: 52.03 at.%) were determined. (C) 2008 Elsevier Inc. All rights reserved.
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