期刊
LETTERS IN ORGANIC CHEMISTRY
卷 8, 期 6, 页码 416-422出版社
BENTHAM SCIENCE PUBL LTD
DOI: 10.2174/157017811796064467
关键词
Vinylphosphonate; phosphonation; triethyl phosphite; B-nitro-alkene
Phosphonation of beta-nitro-alkene with triethyl phosphite was achieved under microwave irradiation using CH2Cl (2) as the solvent in the absence of catalyst with moderate to high yields (up to 90%). This method of formation of carbon-phosphor bonds is simple, mild, convenient and effective. Synchronously, a number of vinylphosphonates derivatives were synthesized and evaluated biologically preliminary.
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