Novel reproducible preparations of gold nanoparticles capped by aminoalcohols have been set up by reduction of HAuCl(4) with NaBH(4) in aqueous solution. The characterization of Au@aminoalcohol nanoparticles performed by (1)H NMR, ATR-FTIR, UV-vis spectroscopies, and TEM microscopy highlighted the binding site and the nature of the Au-NH bond.
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