期刊
JPC-JOURNAL OF PLANAR CHROMATOGRAPHY-MODERN TLC
卷 24, 期 3, 页码 196-200出版社
RESEARCH INST MEDICINAL PLANTS
DOI: 10.1556/JPC.24.2011.3.3
关键词
Benzoxazine; Reversed-phase thin-layer chromatography (RP-TLC); Lipophilicity; R(M); log P
资金
- Ministry of Education of the Czech Republic [MSM 0021620822, SVV-2010-261-001]
- Grant Agency of Charles University [GAUK 11809/2009/B-CH/FAF]
Experimental R(M) values of a series of 3-(4-alkylphenyl)-4-thioxo-2H-1,3-benzoxazine-2(3H)-ones and 3-(4-alkylphenyl)-2H-1,3-benzoxazine-2,4(3H)-dithiones were obtained by a reversed-phase TLC system. The mobile phase was a phosphate buffer with volume fractions of acetone between 80 and 60%. The retention constants R(M)(0) were compared with the partition coefficients calculated using different software products. The lipophilicity contributions of the sub-stituents were compared with the pi constants.
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