期刊
JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
卷 92, 期 3, 页码 945-951出版社
SPRINGER
DOI: 10.1007/s10973-007-8546-1
关键词
characterization; heavier lanthanides; 2-methoxybenzoate; thermal behaviour
Solid-state Ln(L)(3) compounds, where Ln stands for trivalent Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu and Y and L is 2-methoxybenzoate have been synthesized. Simultaneous thermogravimetry and differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results provided information on the composition, dehydration, coordination mode, structure, thermal behaviour and thermal decomposition.
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