期刊
JOURNAL OF THE CHINESE CHEMICAL SOCIETY
卷 58, 期 1, 页码 94-100出版社
CHINESE CHEMICAL SOC
DOI: 10.1002/jccs.201190064
关键词
Aryl iodide; Diaryl sulfide; Ligand; Copper iodide; Cross-coupling; Microwave heating
资金
- National Science Council of the Republic of China, Taiwan [NSC96-2320-B002-017]
The construction of diaryl sulfides through the cross-coupling of aryl iodides and thiols in microwave heating is described. By using this method, a variety of diaryl sulfides can be prepared in a mild condition and in high yields. Deactivated 4-nitrothiophenol was effective to afford the product in 94% yield. Sterically hindered ortho-substituted aryl iodides or thiophenols provided diaryl sulfides effectively by this microwave-assisted coupling reaction.
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