期刊
JOURNAL OF THE BRAZILIAN CHEMICAL SOCIETY
卷 19, 期 5, 页码 856-861出版社
SOC BRASILEIRA QUIMICA
DOI: 10.1590/S0103-50532008000500008
关键词
biodiesel; microemulsion; FAES; sodium and potassium
A method for the determination of Na and K in biodiesel, from different vegetable oils, is proposed. The advantages of the FAES were combined with the simplicity of microemulsion preparation and calibration using aqueous standards. Microemulsions were prepared by mixing biodiesel samples with n-propanol and aqueous acid solution, which allowed the use of inorganic aqueous standards for the calibration. Sample introduction through discrete aspiration (DA) or by continuous aspiration (CA) were compared, presenting similar LODs, in the order of 0.1 mu g g(-1) for both analytes, adequate to the established limits in the Brazilian legislation. The accuracy of the method was checked through recovery tests, with results between 83% and 120%, and through the comparison of the results with those obtained by ICP OES.
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