4.8 Article

Ni(II)-Catalyzed Oxidative Coupling between C(sp2)-H in Benzamides and C(sp3)-H in Toluene Derivatives

期刊

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
卷 136, 期 44, 页码 15509-15512

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AMER CHEMICAL SOC
DOI: 10.1021/ja5095342

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资金

  1. MEXT
  2. JST
  3. JSPS Research Fellowship for Young Scientists
  4. Grants-in-Aid for Scientific Research [14J03693, 22105002, 22105001] Funding Source: KAKEN

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Oxidative coupling between C((sp2)))-H bonds and C((sp3)))-H bonds is achieved by the Ni(II)-catalyzed reaction of benzamides containing an 8-aminoquinoline moiety as the directing group with toluene derivatives in the presence of heptafluoroisopropyl iodide as the oxidant. The method has a broad scope and shows high functional group compatibility. Toluene derivatives can be used as the coupling partner in an unreactive solvent.

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