期刊
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
卷 135, 期 46, 页码 17508-17513出版社
AMER CHEMICAL SOC
DOI: 10.1021/ja409014v
关键词
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资金
- Scripps Research Institute
- NIH (NIGMS) [2R01GM084019]
- Bristol-Myers Squibb Co.
- US EPA (STAR predoctoral fellowship) [FP917296-01-0]
- Swiss National Science Foundation
A protocol for the Pd(II)-catalyzed ortho-C-H alkylation of phenylacetic and benzoic acids using alkylboron reagents is disclosed. Monoprotected amino acid ligands (MPAA) were found to significantly promote reactivity. Both potassium alkyltrifluoroborates and alkylboronic acids were compatible coupling partners. The possibility of a radical alkyl transfer to Pd(II) was also investigated.
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