期刊
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
卷 135, 期 9, 页码 3387-3390出版社
AMER CHEMICAL SOC
DOI: 10.1021/ja400648w
关键词
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资金
- NSF under the CCI Center for Selective C-H Functionalization [CHE-1205646]
- Scripps Research Institute
- Sigma-Aldrich
- Bristol-Myers-Squibb
- Agency for Science, Technology and Research (A*STAR) Singapore
- Division Of Chemistry
- Direct For Mathematical & Physical Scien [1205646] Funding Source: National Science Foundation
The alkynylation of beta-C(sp(3))-H bonds in aliphatic amides with alkynyl halides has been enabled using Pd(0)/N-heterocyclic carbene (NHC) and Pd(0)/phosphine (PR3) catalysts. This is the first example of utilizing [AlkynylPd(II)L-n] complexes to activate C(sp(3))-H bonds.
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