期刊
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
卷 133, 期 39, 页码 15308-15311出版社
AMER CHEMICAL SOC
DOI: 10.1021/ja2064395
关键词
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资金
- National Institutes of Health [R01 GM08525]
- John M. Witt Jr. Fellowship
- Alexander von Humboldt Foundation
Catalytic asymmetric sulfenylation of double bonds has been achieved using a BINAM-based phosphoramide catalyst and an electrophilic sulfur source. Simple alkenes as well as styrenes afforded sulfenylated tetrahydrofurans and tetrahydropyrans by closure with pendant hydroxyl or carboxyl groups. Intermolecular thiofunctionalizations were also achieved with simple alcohols or carboxylic acids as the nucleophiles.
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